• editor@ijmra.in
  • ISSN[Online] : 2643-9875  ||  ISSN[Print] : 2643-9840

Volume 07 Issue 07 July 2024

Prepare Aromatic Derivatives of Nanosheets by a Specially Designed Electrolytic Cell
1Ghazwan H. Abd AL-Wahab, 2Tariq B. Mahmood, 3Ammar S. Mohammed
1Tikrit University
2Salah al-Din Education Directorate
3Kirkuk University
DOI : https://doi.org/10.47191/ijmra/v7-i07-05

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ABSTRACT:

This research includes the preparation of aromatic derivatives of nanosheets by the electrochemical method ArCBG (I, II) by a specially designed electrolytic cell (SDEC) in two steps: The first step: prepare diazonium salts by using one of the amines (4-Aminobenzoic acid, 4 e) -Aminophenazonand second step: Preparation of highly aromatic nanosheets by used CBG nano-carbon was dissolved in 800 ml of distilled water and then placed in an ultrasonic bath.The compounds were diagnosed us-ing FT-IR, XRD, FESEM and AFM.

KEYWORDS:

Nano, Electrolytic Cell, Electrochemical, Graphene.

REFERENCES
1) Sun, X., Liu, Z., Welsher, K., Robinson, J. T., Goodwin, A., Zaric, S., & Dai, H. (2008). Nano-graphene oxide for cellular imaging and drug delivery. Nano research, 1(3), 203-212.

2) Gonçalves, G., Vila, M., Portolés, M. T., Vallet‐Regi, M., Gracio, J., & Marques, P. A. A. (2013). Nano‐graphene oxide: a potential multifunctional platform for cancer therapy. Advanced healthcare materials, 2(8), 1072-1090.

3) Seabra, A. B., Paula, A. J., de Lima, R., Alves, O. L., & Durán, N. (2014). Nanotoxicity of graphene and graphene oxide. Chemical research in toxicology, 27(2), 1

4) Tian, B., Wang, C., Zhang, S., Feng, L., & Liu, Z. (2011). Photothermally enhanced photodynamic therapy delivered by nano-graphene oxide. ACS nano, 5(9), 7000-7009.

5) Chuah, S., Pan, Z., Sanjayan, J. G., Wang, C. M., & Duan, W. H. (2014). Nano reinforced cement and concrete compo-sites and new perspective from graphene oxide. Construction and Building materials, 73, 113-124.

6) Luo, J., Cote, L. J., Tung, V. C., Tan, A. T., Goins, P. E., Wu, J., & Huang, J. (2010). Graphene oxide nanocolloids. Journal of the American Chemical Society, 132(50), 17667-17669.

7) Wang, Y., Li, Z., Wang, J., Li, J., & Lin, Y. (2011). Graphene and graphene oxide: biofunctionalization and applications in biotechnology. Trends in biotechnology, 29(5), 205-212.

8) Cheng, M., Yang, R., Zhang, L., Shi, Z., Yang, W., Wang, D., ... & Zhang, G. (2012). Restoration of graphene from gra-phene oxide by defect repair. Carbon, 50(7), 2581-2587.

9) Yang, K., Gong, H., Shi, X., Wan, J., Zhang, Y., & Liu, Z. (2013). In vivo biodistribution and toxicology of functionalized nano-graphene oxide in mice after oral and intraperitoneal administration. Biomaterials, 34(11), 2787-2795.

10) Pei, X., Zhu, Z., Gan, Z., Chen, J., Zhang, X., Cheng, X., ... & Wang, J. (2020). PEGylated nano-graphene oxide as a nanocarrier for delivering mixed anticancer drugs to improve anticancer activity. Scientific reports, 10(1), 1-15.

11) Rahmanian, N., Hamishehkar, H., Dolatabadi, J. E. N., & Arsalani, N. (2014). Nano graphene oxide: a novel carrier for oral delivery of flavonoids. Colloids and Surfaces B: Biointerfaces, 123, 331-338.

12) Perrozzi, F., Prezioso, S., & Ottaviano, L. (2014). Graphene oxide: from fundamentals to applications. Journal of Phys-ics: Condensed Matter, 27(1), 013002.

13) Ray, S. C. (2015). Application and uses of graphene oxide and reduced graphene oxide. Applications of graphene and graphene-oxide based nanomaterials, 1.

14) Jang, S. C., Kang, S. M., Lee, J. Y., Oh, S. Y., Vilian, A. E., Lee, I., & Huh, Y. S. (2018). Nano-graphene oxide composite for in vivo imaging. International journal of nanomedicine, 13, 221.

15) Dong, H., Zhao, Z., Wen, H., Li, Y., Guo, F., Shen, A., ... & Shi, D. (2010). Poly (ethylene glycol) conjugated nano-graphene oxide for photodynamic therapy. Science China Chemistry, 53(11), 2265-2271.

16) Ryoo, S. R., Lee, J., Yeo, J., Na, H. K., Kim, Y. K., Jang, H., ... & Min, D. H. (2013). Quantitative and multiplexed microRNA sensing in living cells based on peptide nucleic acid and nano graphene oxide (PANGO). ACS nano, 7(7), 5882-5891.

17) Delekta, S. S., Adolfsson, K. H., Erdal, N. B., Hakkarainen, M., Östling, M., & Li, J. (2019). Fully inkjet printed ultrathin microsupercapacitors based on graphene electrodes and a nano-graphene oxide electrolyte. Nanoscale, 11(21), 10172-10177.

18) Hu, X., Yu, Y., Wang, Y., Zhou, J., & Song, L. (2015). Separating nano graphene oxide from the residual strong-acid fil-trate of the modified Hummers method with alkaline solution. Applied Surface Science, 329, 83-86.

19) Wen, H., Dong, C., Dong, H., Shen, A., Xia, W., Cai, X., ... & Shi, D. (2012). Engineered redox‐responsive PEG detach-ment mechanism in PEGylated nano‐graphene oxide for intracellular drug delivery. Small, 8(5), 760-769.

20) Chung, C., Kim, Y. K., Shin, D., Ryoo, S. R., Hong, B. H., & Min, D. H. (2013). Biomedical applications of graphene and graphene oxide. Accounts of chemical research, 46(10), 2211-2224.

21) Yang, D., Feng, L., Dougherty, C. A., Luker, K. E., Chen, D., Cauble, M. A., & Hong, H. (2016). In vivo targeting of meta-static breast cancer via tumor vasculature-specific nano-graphene oxide. Biomaterials, 104, 361-371.

22) Adeel, M., Bilal, M., Rasheed, T., Sharma, A., & Iqbal, H. M. (2018). Graphene and graphene oxide: Functionalization and nano-bio-catalytic system for enzyme immobilization and biotechnological perspective. International journal of biological macromolecules, 120, 1430-1440.

23) Jabar, S. A., Hussein, A. L., Dalaf, A. H., & Aboud, H. S. (2020). Synthesis and Characterization of Azetidine and Oxaze-pine Compounds Using Ethyl-4-((4-Bromo Benzylidene) Amino) Benzoate as Precursor and Evalution of Their Biologi-cal Activity. Journal of Education and Scientific Studies, 5(16).

24) Dalaf, A. H. (2018). Synthesis and Characterization of Some Quartet and Quinary Hetero cyclic Rings Compounds by Traditional Method and Microwave Routes Method and Evaluation of Their Biological Activity. M.Sc. Thesis, Tikrit University, Tikrit, Iraq: 1-94 pp.

25) Dalaf, A. H., & Jumaa, F. H. (2018). Synthesis, Characterization of some 1,3-Oxazepane -4,7-Dione by Traditional and Microwave routes method and evaluation of their biological activity. Al-utroha for Pure Science. (8): 93-108.

26) Dalaf, A. H., Jumaa, F. H., & Jabbar, S. A. S. (2018). Synthesis and Characterization of some 2, 3-dihydroquinozoline and evaluation of their biological activity. Tikrit Journal of Pure Science, 23(8): 66-67.

27) Salwa, A. J., Ali, L. H., Adil, H. D., Hossam, S. A. (2020). Synthesis and Characterization of Azetidine and Oxazepine Compounds Using Ethyl-4-((4-Bromo Benzylidene) Amino) Benzoate as Precursor and Evalution of Their Biological Ac-tivity. Journal of Education and Scientific Studies, ISSN: 24134732. 16(5): 39-52.

28) Dalaf, A. H., & Jumaa, F. H. (2020). Synthesis, Identification and Assess the Biological and Laser Efficacy of New Com-pounds of Azetidine Derived from Benzidine. Muthanna Journal of Pure Science (MJPS), 7(2):12-25.

29) Saleh, R. H., Rashid, W. M., Dalaf, A. H., Al-Badrany, K. A., & Mohammed, O. A. (2020). Synthesis of Some New Thiazol-idinone Compounds Derived from Schiff Bases Compounds and Evaluation of Their Laser and Biological Efficacy. Ann Trop & Public Health, 23(7): 1012-1031.

30) Yass, I. A., Aftan, M. M., Dalaf, A. H., & Jumaa, F. H. (Nov. 2020). Synthesis and Identification of New Derivatives of Bis-1,3-Oxazepene and 1,3-Diazepine and Assess the Biological and Laser Efficacy for Them. The Second International & The Fourth Scientific Conference of College of Science – Tikrit University. (P4): 77-87.

31) Salih, B. D., Dalaf, A. H., Alheety, M. A., Rashed, W. M., & Abdullah, I. Q. (2021). Biological activity and laser efficacy of new Co (II), Ni (II), Cu (II), Mn (II) and Zn (II) complexes with phthalic anhydride. Materials Today: Proceedings, 43, 869-874.

32) Aftan, M. M., Jabbar, M. Q., Dalaf, A. H., & Salih, H. K. (2021). Application of biological activity of oxazepine and 2-azetidinone compounds and study of their liquid crystalline behavior. Materials Today: Proceedings, 43, 2040-2050.

33) Aftan, M. M., Talloh, A. A., Dalaf, A. H., & Salih, H. K. (2021). Impact para position on rho value and rate constant and study of liquid crystalline behavior of azo compounds. Materials Today: Proceedings.

34) Aftan, M. M., Toma, M. A., Dalaf, A. H., Abdullah, E. Q., & Salih, H. K. (2021). Synthesis and Characterization of New Azo Dyes Based on Thiazole and Assess the Biological and Laser Efficacy for Them and Study their Dyeing Application. Egyptian Journal of Chemistry, 64(6), 2903-2911.

35) Khalaf, S. D., Ahmed, N. A. A. S., & Dalaf, A. H. (2021). Synthesis, characterization and biological evaluation (antifungal and antibacterial) of new derivatives of indole, benzotriazole and thioacetyl chloride. Materials Today: Proceedings.‏47(17), 6201-6210.

36) Dalaf, A. H., Jumaa, F. H., & Salih, H. K. (2021). Preparation, Characterization, Biological Evaluation and Assess Laser Efficacy for New Derivatives of Imidazolidin-4-one. International Research Journal of Multidisciplinary Technovation, 3(4), 41-51.

37) Dalaf, A. H., Jumaa, F. H., & Salih, H. K. (2021). MULTIDISCIPLINARY TECHNOVATION. Red, 15(A2), C44H36N10O8.

38) Dalaf, A. H., Jumaa, F. H., Aftana, M. M., Salih, H. K., & Abd, I. Q. (2022). Synthesis, Characterization, Biological Evalua-tion, and Assessment Laser Efficacy for New Derivatives of Tetrazole. In Key Engineering Materials (Vol. 911, pp. 33-39). Trans Tech Publications Ltd.

39) Lee, J., Yim, Y., Kim, S., Choi, M. H., Choi, B. S., Lee, Y., & Min, D. H. (2016). In-depth investigation of the interaction be-tween DNA and nano-sized graphene oxide. Carbon, 97, 92-98.
Volume 07 Issue 07 July 2024

There is an Open Access article, distributed under the term of the Creative Commons Attribution – Non Commercial 4.0 International (CC BY-NC 4.0) (https://creativecommons.org/licenses/by-nc/4.0/), which permits remixing, adapting and building upon the work for non-commercial use, provided the original work is properly cited.


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